The first total synthesis of a glycolipid from S. pneumoniae and the biological re-evaluation of their immunological activity

Submitter and Co-author information

Khushali Parikh Miss, University of WindsorFollow

Standing

Undergraduate

Type of Proposal

Oral Presentation

Faculty

Faculty of Science

Proposal

Invariant natural killer T cells (iNKT), a subclass of white blood cells, are responsible for the production of non-specific cytokines which induce a systemic uncontrolled immune response. They are distinctive in having a monospecific T-cell receptor that recognizes glycolipid antigens. The natural antigen was not identified until quite recently, when putative targets were isolated from S. pneumoniae. A bioactive fraction was identified from the extract: a disaccharide moiety attached to diacylglycerol (DAG). The glycolipid antigen reportedly activated iNKT cells. However, these tests were carried out using very small amounts of isolated glycolipids, as a result it is impossible to ascertain whether the activity was due to this compound or to some minor impurity. There was also insufficient evidence to conclusively confirm the proposed structure. Consequently, we recently synthesized the glycolipid to both confirm the structural assignment and to provide a useful chemical probe for immunologists. This presentation will discuss this S. pneumoniae glycolipid, its total synthesis, and our surprising re-evaluation of their immunological activity.

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The first total synthesis of a glycolipid from S. pneumoniae and the biological re-evaluation of their immunological activity

Invariant natural killer T cells (iNKT), a subclass of white blood cells, are responsible for the production of non-specific cytokines which induce a systemic uncontrolled immune response. They are distinctive in having a monospecific T-cell receptor that recognizes glycolipid antigens. The natural antigen was not identified until quite recently, when putative targets were isolated from S. pneumoniae. A bioactive fraction was identified from the extract: a disaccharide moiety attached to diacylglycerol (DAG). The glycolipid antigen reportedly activated iNKT cells. However, these tests were carried out using very small amounts of isolated glycolipids, as a result it is impossible to ascertain whether the activity was due to this compound or to some minor impurity. There was also insufficient evidence to conclusively confirm the proposed structure. Consequently, we recently synthesized the glycolipid to both confirm the structural assignment and to provide a useful chemical probe for immunologists. This presentation will discuss this S. pneumoniae glycolipid, its total synthesis, and our surprising re-evaluation of their immunological activity.